1,3-diferrocenyl-1-phenylallenium tetrafluoroborate

Base Information

Chemical Name:1,3-diferrocenyl-1-phenylallenium tetrafluoroborate
CAS No.:672958-77-9
Molecular Formula:BF₄*C₂₉H₂₃Fe₂
Molecular Weight:570
Hs Code.:

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Chemical Property of 1,3-diferrocenyl-1-phenylallenium tetrafluoroborate

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Technology Process of 1,3-diferrocenyl-1-phenylallenium tetrafluoroborate

There total 1 articles about 1,3-diferrocenyl-1-phenylallenium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.2%

: tetrafluoroboric acid

: 77781-63-6
1,3-Diferrocenyl-1-phenyl-propinol

: 672958-77-9
1,3-diferrocenyl-1-phenylallenium tetrafluoroborate

Guidance literature:: In diethyl ether; byproducts: water; 54% ethereal HBF4 was added under Ar to an ether soln. of the alcohol, the resulting suspn. was stirred for 10 min; ppt. was filtd. off, washed with Et2O, dried in vacuo; elem. anal.;

Reference yield: 27.8%

: 672958-77-9
1,3-diferrocenyl-1-phenylallenium tetrafluoroborate

: 591-51-5
phenyllithium

: 1,3-diphenyl-1,3-diferrocenylallene

: 1,3,4,6-tetraferrocenyl-1,4-diphenylhexa-1,2-dien-5-yne

Guidance literature:: In diethyl ether; cyclohexane; benzene; Sonication; a soln. of PhLi in cyclohexane/ether was added at 10°C under Ar to the BF4-salt in benzene, the mixt. was sonicated in an ultrasound cleaning bath for 1 h and stirred at room temp. for an addnl. hour; filtd. through a short alumina plug, evapd. in vacuo, residue was chromd. on basic alumina (eluent 2:1 hexane-ether); elem. anal.;