1,3-Diferrocenyl-1-phenyl-propinol

Base Information

Chemical Name:1,3-Diferrocenyl-1-phenyl-propinol
CAS No.:77781-63-6
Molecular Formula:C₂₉H₂₄Fe₂O
Molecular Weight:500.203
Hs Code.:

Synonyms:1,3-Diferrocenyl-1-phenyl-propinol

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Chemical Property of 1,3-Diferrocenyl-1-phenyl-propinol

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Technology Process of 1,3-Diferrocenyl-1-phenyl-propinol

There total 1 articles about 1,3-Diferrocenyl-1-phenyl-propinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1271-47-2
ferroceneacetylene

: 1272-44-2
benzoylferrocene

: 77781-63-6
1,3-Diferrocenyl-1-phenyl-propinol

Guidance literature:: With n-butyllithium; In diethyl ether; benzoylferrocene/ether soln. addn. during 20 min to ethynylferrocene/n-butyllithium/ether soln.; 2 h; all react. under Ar; chromd. with benzene (starting materials); elution with ether;
DOI:10.1007/BF00906246

Reference yield: 85.0%

: 77781-63-6
1,3-Diferrocenyl-1-phenyl-propinol

: 77781-64-7
1,3-Diferrocenyl-1-phenyl-propin

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; 30 min mixing at room temp. (Ar); chromd. (benzene);
DOI:10.1007/BF00906246

Reference yield: 78.2%

: tetrafluoroboric acid

: 77781-63-6
1,3-Diferrocenyl-1-phenyl-propinol

: 672958-77-9
1,3-diferrocenyl-1-phenylallenium tetrafluoroborate

Guidance literature:: In diethyl ether; byproducts: water; 54% ethereal HBF4 was added under Ar to an ether soln. of the alcohol, the resulting suspn. was stirred for 10 min; ppt. was filtd. off, washed with Et2O, dried in vacuo; elem. anal.;