C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾

Base Information

Chemical Name:C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾
CAS No.:97037-94-0
Molecular Formula:C₂₈H₂₂N₃O₂S*Li
Molecular Weight:471.509
Hs Code.:

C<sub>28</sub>H<sub>22</sub>N<sub>3</sub>O<sub>2</sub>S<sup>(1-)</sup>*Li<sup>(1+)</sup>

Synonyms:

Suppliers and Price of C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾

There total 4 articles about C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-44-8
anthracen-9(10H)-one

: 97037-94-0
C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / diethyl ether / 24 h / Heating

2: 30 percent / Br₂ / CCl₄ / 3 h

3: 77 percent / 3-methylbutylnitrite / 1,2-dimethoxy-ethane / 1.) 15 min, reflux, 2.) 0.75 h, reflux, 3.) 1.5 h, reflux

4: 1.) 1.78 M BuLi / 1.) ether, hexane, 4 h, -30 deg C, 2.) ether, 2.5 h

With n-butyllithium; bromine; isopentyl nitrite; In tetrachloromethane; 1,2-dimethoxyethane; diethyl ether;

Reference yield:

: 779-02-2
9-methylanthracene

: 97037-94-0
C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / Br₂ / CCl₄ / 3 h

2: 77 percent / 3-methylbutylnitrite / 1,2-dimethoxy-ethane / 1.) 15 min, reflux, 2.) 0.75 h, reflux, 3.) 1.5 h, reflux

3: 1.) 1.78 M BuLi / 1.) ether, hexane, 4 h, -30 deg C, 2.) ether, 2.5 h

With n-butyllithium; bromine; isopentyl nitrite; In tetrachloromethane; 1,2-dimethoxyethane;

Reference yield:

: 23674-17-1
9-bromo-10-methylanthracene

: 97037-94-0
C₂₈H₂₂N₃O₂S^(1-)*Li⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / 3-methylbutylnitrite / 1,2-dimethoxy-ethane / 1.) 15 min, reflux, 2.) 0.75 h, reflux, 3.) 1.5 h, reflux

2: 1.) 1.78 M BuLi / 1.) ether, hexane, 4 h, -30 deg C, 2.) ether, 2.5 h

With n-butyllithium; isopentyl nitrite; In 1,2-dimethoxyethane;