[Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)]

Base Information

Chemical Name:[Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)]
CAS No.:769968-25-4
Molecular Formula:C₂₄H₁₉IN₄Pd
Molecular Weight:596.766
Hs Code.:

[Pd(C<sub>6</sub>H<sub>4</sub>N=C=N(C<sub>6</sub>H<sub>4</sub>Me-4)-2)I(2,2'-bipyridine)]

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Chemical Property of [Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)]

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Technology Process of [Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)]

There total 1 articles about [Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 366-18-7
[2,2]bipyridinyl

: Pd2(dba)4

: 769968-23-2
N-((2-iodophenylimino)methylene)-4-methylbenzenamine

: 769968-25-4
[Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)]

Guidance literature:: In toluene; (N2); stirring a mixt. of palladium complex and bpy in toluene for 10 min at 0°C, addn. of ligand and toluene, stirring for 16 h with warming to room temp.; addn. of CH2Cl2, filtration over MgSO4, evapn., trituration with Et2O, filtration, washing with Et2O, drying; elem. anal.;
DOI:10.1021/om049580p

Reference yield: 90.0%

: 3978-81-2
4-tert-butylpyridine

: 769968-25-4
[Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)]

: 73491-36-8
thallium(I) triflate

: 769968-30-1
[Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)(4-tert-butylpyridine)(2,2'-bipyridine)]triflate

Guidance literature:: In acetone; byproducts: TlI; (N2); addn. of ligand and thallium salt to a suspn. of palladium complexin acetone, stirring for 10 min; filtration through Celite, evapn., trituration with Et2O, filtration, washing ppt. with Et2O, drying in vac. overnight; elem. anal.;
DOI:10.1021/om049580p

Reference yield: 75.0%

: 769968-25-4
[Pd(C₆H₄N=C=N(C₆H₄Me-4)-2)I(2,2'-bipyridine)]

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 769968-31-2
trans-[Pd(3-(2,6-dimethylphenyl)-2-[(4-methylphenyl)imino]-2,3-dihydroquinazolin-4-yl)I(2,6-dimethylphenylisonitrile)2]

Guidance literature:: In dichloromethane; byproducts: 2,2'-bipyridine; react. palladium complex with ligand in CH2Cl2 for 30 min; filtration through Celite, evapn., addn. of Et2O, filtration, washing with Et2O, drying;
DOI:10.1021/om049580p