Technology Process of C11H16O3
There total 12 articles about C11H16O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
dimethyl sulfoxide;
Ambient temperature;
DOI:10.1248/cpb.32.805
- Guidance literature:
-
Multi-step reaction with 10 steps
1: acetic anhydride / 140 °C
2: 78 percent / NaBH4 / H2O; tetrahydrofuran
3: Jones oxidation
4: 83 percent / acetalization
5: 1.) diisobutylaluminum hydride / 2.) toluene, 100 deg C
6: K2CO3 / methanol / 50 °C
7: LiAlH4 / diethyl ether
8: tosylation
9: 98 percent / NaI / hexamethylphosphoric acid triamide
10: t-BuOK / dimethylsulfoxide / Ambient temperature
With
sodium tetrahydroborate; lithium aluminium tetrahydride; potassium tert-butylate; diisobutylaluminium hydride; potassium carbonate; sodium iodide;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; water; acetic anhydride; dimethyl sulfoxide;
DOI:10.1248/cpb.32.805
- Guidance literature:
-
Multi-step reaction with 10 steps
1: metaphospholic acid / 200 °C
2: 78 percent / NaBH4 / H2O; tetrahydrofuran
3: Jones oxidation
4: 83 percent / acetalization
5: 1.) diisobutylaluminum hydride / 2.) toluene, 100 deg C
6: K2CO3 / methanol / 50 °C
7: LiAlH4 / diethyl ether
8: tosylation
9: 98 percent / NaI / hexamethylphosphoric acid triamide
10: t-BuOK / dimethylsulfoxide / Ambient temperature
With
sodium tetrahydroborate; lithium aluminium tetrahydride; potassium tert-butylate; diisobutylaluminium hydride; potassium carbonate; meta-phosphoric acid; sodium iodide;
In
tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; water; dimethyl sulfoxide;
DOI:10.1248/cpb.32.805
