zinc 5,17-bis[meso-(3-hydroxyphenyl)tetramethyltetraethylporphyrinate]-25,27-dimethoxy-26,28-crown[6]-calix[4]arene, 1,3-alternate

Base Information

• Chemical Name: zinc 5,17-bis[meso-(3-hydroxyphenyl)tetramethyltetraethylporphyrinate]-25,27-dimethoxy-26,28-crown[6]-calix[4]arene, 1,3-alternate
• CAS No.: 1308679-35-7
• Molecular Formula: C₁₁₆H₁₂₂N₈O₁₀Zn₂
• Molecular Weight: 1919.07

Synonyms:

Chemical Property of zinc 5,17-bis[meso-(3-hydroxyphenyl)tetramethyltetraethylporphyrinate]-25,27-dimethoxy-26,28-crown[6]-calix[4]arene, 1,3-alternate

Chemical Property:

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Technology Process of zinc 5,17-bis[meso-(3-hydroxyphenyl)tetramethyltetraethylporphyrinate]-25,27-dimethoxy-26,28-crown[6]-calix[4]arene, 1,3-alternate

There total 1 articles about zinc 5,17-bis[meso-(3-hydroxyphenyl)tetramethyltetraethylporphyrinate]-25,27-dimethoxy-26,28-crown[6]-calix[4]arene, 1,3-alternate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

5,17-bis[meso-(3-hydroxyphenyl)tetramethyltetraethylporphyrin]-25,27-dimethoxy-26,28-crown[6]-calix[4]arene, 1,3-alternate + zinc diacetate (557-34-6) → zinc 5,17-bis[meso-(3-hydroxyphenyl)tetramethyltetraethylporphyrinate]-25,27-dimethoxy-26,28-crown[6]-calix[4]arene, 1,3-alternate (1308679-35-7)

Guidance literature:

In N,N-dimethyl-formamide; to soln. of ligand in DMF was added excess (1:10) of Zn salt; mixt. refluxed for 30 min; cooled; diluted with H2O; ppt. filtered off; ppt. dried; subjected to chromy. on aluminum oxide (CH2Cl2-C6H14, 1:1 as eluent); solvent distd. off (vac.); recrystd. (CH2Cl2-CH3OH, 1:1);

DOI:10.1134/S1070363211030273

upstream raw materials:

zinc diacetate

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