(Z) ethyl 2-(tert-butyldimethylsilyloxy)cyclohexylidene carboxylate

Base Information

Chemical Name:(Z) ethyl 2-(tert-butyldimethylsilyloxy)cyclohexylidene carboxylate
CAS No.:78707-61-6
Molecular Formula:C₁₆H₃₀O₃Si
Molecular Weight:298.498
Hs Code.:

Synonyms:

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Chemical Property of (Z) ethyl 2-(tert-butyldimethylsilyloxy)cyclohexylidene carboxylate

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Technology Process of (Z) ethyl 2-(tert-butyldimethylsilyloxy)cyclohexylidene carboxylate

There total 2 articles about (Z) ethyl 2-(tert-butyldimethylsilyloxy)cyclohexylidene carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74173-08-3
2-(tert-Butyldimethylsilyloxy)-1-cyclohexanon

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 78707-61-6
(Z) ethyl 2-(tert-butyldimethylsilyloxy)cyclohexylidene carboxylate

: 78707-59-2
(E)-2-(tert-butyldimethylsiloxy)<(1-carboethoxy)methylidene>cyclohexane

Guidance literature:: With benzoic acid; In toluene; Yield given. Yields of byproduct given; Heating;
DOI:10.1016/S0040-4039(01)90381-8

Reference yield:

: 4071-88-9
trimethylsilanyl-acetic acid ethyl ester

: 74173-08-3
2-(tert-Butyldimethylsilyloxy)-1-cyclohexanon

: 78707-61-6
(Z) ethyl 2-(tert-butyldimethylsilyloxy)cyclohexylidene carboxylate

: 78707-59-2
(E)-2-(tert-butyldimethylsiloxy)<(1-carboethoxy)methylidene>cyclohexane

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 0.5 h, 2.) room temp.;
DOI:10.1016/S0040-4039(01)90381-8