Technology Process of C27H34N2O12
There total 5 articles about C27H34N2O12 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
dichloromethane;
at 20 ℃;
for 24h;
DOI:10.1021/jm3009713
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap / pyridine / 24 h / 20 °C / Cooling with ice
2: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2.5 h / 0 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / ethanol / 0.17 h
4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 24 h / 20 °C
With
dmap; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
pyridine; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm3009713
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2.5 h / 0 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / ethanol / 0.17 h
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 24 h / 20 °C
With
trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jm3009713
