1-(2-Bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine

Base Information

• Chemical Name: 1-(2-Bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine
• CAS No.: 4880-96-0
• Molecular Formula: C14H11 Br N4 O4
• Molecular Weight: 379.17
• DSSTox Substance ID: DTXSID90964122
• Mol file: 4880-96-0.mol

Synonyms:4880-96-0;DTXSID90964122;1-(2-bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine

Chemical Property of 1-(2-Bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine

Chemical Property:

• Vapor Pressure: 7.51E-10mmHg at 25°C
• Boiling Point: 492.7°Cat760mmHg
• Flash Point: 251.8°C
• Density: 1.62g/cm³
• XLogP3: 5.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 4
• Exact Mass: 377.99637
• Heavy Atom Count: 23
• Complexity: 457

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NNC2=C(C=C(C=C2)[N+](=O)[O-])[N+](=O)[O-])CBr

Technology Process of 1-(2-Bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine

There total 2 articles about 1-(2-Bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

α-bromoacetophenone (70-11-1) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → 1-(2-bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine (4880-96-0)

Guidance literature:

With acetic acid; In methanol; at 20 ℃; for 24h;

DOI:10.1016/j.tetlet.2021.153414

Reference yield:

→ 1-(2-bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine (4880-96-0)

Guidance literature:

Bhdl. v. Acetophenon-<2.4-dinitro-phenylhydrazon> m. Brom , Tetrachlormethan ,(UV-Bestr.?);

Reference yield: 94.0%

2,5-dimethylfuran (625-86-5) + 1-(2-bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine (4880-96-0) → 1-(2,4-dinitrophenyl)-4a,6-dimethyl-3-phenyl-1,4,4a,7a-tetrahydrofuro[3,2-c]pyridazine (61145-18-4)

Guidance literature:

With sodium carbonate; In dichloromethane; at 20 ℃; for 23h;

DOI:10.1002/ejoc.201700453

upstream raw materials:

α-bromoacetophenone

(2,4-dinitro-phenyl)-hydrazine

Downstream raw materials:

1-phenyl-propenone-((Z)-2,4-dinitro-phenylhydrazone)

1-phenyl-propenone-((E)-2,4-dinitro-phenylhydrazone)

C₁₉H₁₈N₄O₆

1-(2,4-dinitrophenyl)-3-phenyl-1,4,4a,7a-tetrahydrofuro[3,2-c]pyridazine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 4880-96-0 1-(2-bromo-1-phenylethylidene)-2-(2,4-dinitrophenyl)hydrazine

Send

Send

Metric Ton KG G Pound L ML

Send

Send