Technology Process of C25H30N6O4
There total 6 articles about C25H30N6O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 60 ℃;
regioselective reaction;
DOI:10.1016/j.bmcl.2011.11.054
- Guidance literature:
-
Multi-step reaction with 4 steps
1: bromine; acetic acid / 18 h / 45 °C
2: 4-methyl-morpholine / N,N-dimethyl acetamide / 0.33 h / 160 °C / Microwave irradiation
3: palladium 10% on activated carbon; ammonium formate / 0.5 h / 75 °C
4: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 °C
With
4-methyl-morpholine; palladium 10% on activated carbon; bromine; ammonium formate; acetic acid; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.054
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 4-methyl-morpholine / N,N-dimethyl acetamide / 0.33 h / 160 °C / Microwave irradiation
2: palladium 10% on activated carbon; ammonium formate / 0.5 h / 75 °C
3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 °C
With
4-methyl-morpholine; palladium 10% on activated carbon; ammonium formate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl acetamide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.11.054
