11,26-dimethyl-2,8,13,17,23,28-hexaoxa-12,27,31,33-tetraazaheptacyclo[22.6.1.1(3,7).1(9,16).1(18,22).0(10,14).0(25,29)]tetratriaconta-1⁽³¹⁾,3⁽³⁴⁾,4,6,9,11,14,16⁽³³⁾,18⁽³²⁾,19,21,24,26,29-tetradecaene-5,20-diol

Base Information

• Chemical Name: 11,26-dimethyl-2,8,13,17,23,28-hexaoxa-12,27,31,33-tetraazaheptacyclo[22.6.1.1(3,7).1(9,16).1(18,22).0(10,14).0(25,29)]tetratriaconta-1⁽³¹⁾,3⁽³⁴⁾,4,6,9,11,14,16⁽³³⁾,18⁽³²⁾,19,21,24,26,29-tetradecaene-5,20-diol
• CAS No.: 1111891-09-8
• Molecular Formula: C₂₆H₁₆N₄O₈
• Molecular Weight: 512.435

Synonyms:

Chemical Property of 11,26-dimethyl-2,8,13,17,23,28-hexaoxa-12,27,31,33-tetraazaheptacyclo[22.6.1.1(3,7).1(9,16).1(18,22).0(10,14).0(25,29)]tetratriaconta-1⁽³¹⁾,3⁽³⁴⁾,4,6,9,11,14,16⁽³³⁾,18⁽³²⁾,19,21,24,26,29-tetradecaene-5,20-diol

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Technology Process of 11,26-dimethyl-2,8,13,17,23,28-hexaoxa-12,27,31,33-tetraazaheptacyclo[22.6.1.1(3,7).1(9,16).1(18,22).0(10,14).0(25,29)]tetratriaconta-1⁽³¹⁾,3⁽³⁴⁾,4,6,9,11,14,16⁽³³⁾,18⁽³²⁾,19,21,24,26,29-tetradecaene-5,20-diol

There total 1 articles about 11,26-dimethyl-2,8,13,17,23,28-hexaoxa-12,27,31,33-tetraazaheptacyclo[22.6.1.1(3,7).1(9,16).1(18,22).0(10,14).0(25,29)]tetratriaconta-1⁽³¹⁾,3⁽³⁴⁾,4,6,9,11,14,16⁽³³⁾,18⁽³²⁾,19,21,24,26,29-tetradecaene-5,20-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

4,6-dichloro-3-methylisoxazolo<4,5-c>pyridine (58315-12-1) + 3,5-dihydroxyphenol (108-73-6) → 5-(6-chloro-3-methylisoxazolo[4,5-c]pyridine-4-yloxy)benzene-1,3-diol (1111891-03-2) + 11,26-dimethyl-2,8,13,17,23,28-hexaoxa-12,27,31,33-tetraazaheptacyclo[22.6.1.1(3,7).1(9,16).1(18,22).0(10,14).0(25,29)]tetratriaconta-1(31),3(34),4,6,9,11,14,16(33),18(32),19,21,24,26,29-tetradecaene-5,20-diol (1111891-09-8) + 11,29-dimethyl-2,8,13,17,23,27-hexaoxa-12,28,31,33-tetraazaheptacyclo[22.6.1.1(3,7).1(9,16).1(18,22).0(10,14).0(26,30)]tetratriaconta-1(30),3(34),4,6,9,11,14,16(33),18(32),19,21,24(31),25,28-tetradecaene-5,20-diol + 7,22,34-trimethyl-4,9,13,19,24,28,31,36,40-nonaoxa-8,23,35,41,43,45-hexa-azadecacyclo[14.14.10.1(3,29).1(5,12).1(14,18).1(20,27).1(32,39).0(6,10).0(21,25).0(33,37)]pentatetraconta-1,3(42),5,7,10,12(45),14,15,17,20,22,25,27(43),29,32,34,37,39(41)octadecaene (1111891-06-5) + 7,25,34-trimethyl-4,9,13,19,23,28,31,36,40-nonaoxa-8,24,35,41,43,45-hexaaza-decacyclo[14.14.10.1(3,29).1(5,12).1(14,18).1(20,27).1(32,39).0(6,10).0(22,26).0(33,37)]pentatetraconta-1,3(42),5,7,10,12(45),14,15,17,20,22(26),24,27(43),29,32,34,37,39(41)octadecaene

Guidance literature:

3,5-dihydroxyphenol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

4,6-dichloro-3-methylisoxazolo<4,5-c>pyridine; In dimethyl sulfoxide; at 120 ℃; for 18h;

DOI:10.1002/ejoc.200800714

upstream raw materials:

4,6-dichloro-3-methylisoxazolo<4,5-c>pyridine

3,5-dihydroxyphenol

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