O²-Methyl-D-glucose-dibenzyldithioacetal

Base Information

• Chemical Name: O²-Methyl-D-glucose-dibenzyldithioacetal
• CAS No.: 908575-86-0
• Molecular Formula: C₂₁H₂₈O₅S₂
• Molecular Weight: 424.582
• Mol file: 908575-86-0.mol

Synonyms:

Chemical Property of O²-Methyl-D-glucose-dibenzyldithioacetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O²-Methyl-D-glucose-dibenzyldithioacetal

There total 4 articles about O²-Methyl-D-glucose-dibenzyldithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O5,O6-isopropylidene-D-glucose-dibenzyldithioacetal (64780-63-8) + methyl iodide (74-88-4) → O2-Methyl-D-glucose-dibenzyldithioacetal (908575-86-0)

Guidance literature:

With diethyl ether; sodium; Erwaermen einer Loesung des Reaktionsprodukts in Aethanol mit wss. HCl;

Reference yield:

D-Glucose-dibenzyldithioacetal (6936-67-0) + methyl iodide (74-88-4) → O4-Methyl-D-glucose-dibenzyldithioacetal + O2-Methyl-D-glucose-dibenzyldithioacetal (908575-86-0)

Guidance literature:

With sodium; copper(II) sulfate; acetone; weitere Reagenzien: Aether u. wss.-aethanol. HCl; Reaktion ueber mehrere Stufen;

DOI:10.1007/BF00903021 DOI:10.1039/jr9350000873

Reference yield:

D-Glucose-dibenzyldithioacetal (6936-67-0) → O2-Methyl-D-glucose-dibenzyldithioacetal (908575-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone; copper (II)-sulfate

2: sodium; diethyl ether / Erwaermen einer Loesung des Reaktionsprodukts in Aethanol mit wss. HCl

With diethyl ether; sodium; copper(II) sulfate; acetone;

upstream raw materials:

O⁵,O⁶-isopropylidene-D-glucose-dibenzyldithioacetal

methyl iodide

D-Glucose-dibenzyldithioacetal

Downstream raw materials:

2-O-Methyl-D-glucose