C₁₇H₃₅NO

Base Information

• Chemical Name: C₁₇H₃₅NO
• CAS No.: 1266666-30-1
• Molecular Formula: C₁₇H₃₅NO
• Molecular Weight: 269.471
• Mol file: 1266666-30-1.mol

Synonyms:

Chemical Property of C₁₇H₃₅NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₃₅NO

There total 6 articles about C₁₇H₃₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-(cyclohexylmethoxy)decan-1-ol (1266666-28-7) → C17H35NO (1266666-30-1)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 0 °C / Reflux; Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C / Reflux; Inert atmosphere

3: water; triphenylphosphine / toluene / 0.5 h / Reflux

With sodium azide; water; triethylamine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; toluene; 3: Staudinger reaction;

DOI:10.1021/jm2001053

Reference yield:

(((10-azidodecyl)oxy)methyl)cyclohexane (1266666-29-8) → C17H35NO (1266666-30-1)

Guidance literature:

With water; triphenylphosphine; In toluene; for 0.5h; Reflux;

DOI:10.1021/jm2001053

Reference yield:

10-(cyclohexylmethoxy)decyl methanesulfonate (1307309-81-4) → C17H35NO (1266666-30-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 20 °C / Reflux; Inert atmosphere

2: water; triphenylphosphine / toluene / 0.5 h / Reflux

With sodium azide; water; triphenylphosphine; In N,N-dimethyl-formamide; toluene; 2: Staudinger reaction;

DOI:10.1021/jm2001053

upstream raw materials:

((dec-9-en-1-yloxy)methyl)cyclohexane

10-(cyclohexylmethoxy)decan-1-ol

(((10-azidodecyl)oxy)methyl)cyclohexane

10-(cyclohexylmethoxy)decyl methanesulfonate

Downstream raw materials:

VPC₁₄₃₁₄₄

1-cyano-N-(10-(cyclohexylmethoxy)decyl)cyclopropanecarboxamide