benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate

Base Information

Chemical Name:benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate
CAS No.:1429913-74-5
Molecular Formula:C₁₈H₂₇N₃O₅
Molecular Weight:365.429
Hs Code.:

Synonyms:

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Chemical Property of benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate

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Technology Process of benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate

There total 6 articles about benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65710-57-8,81306-93-6
3-{[(benzyloxy)carbonyl]amino}-N-(tert-butoxycarbonyl)-L-alanine

: 1429913-74-5
benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / dimethyl sulfoxide / 12 h / 20 °C

2: lithium borohydride / tetrahydrofuran / 1 h / 0 - 20 °C

3: dichloromethane / 12 h / 0 - 20 °C

4: sodium azide / N,N-dimethyl-formamide / 24 h / 50 °C

5: palladium 10% on activated carbon; hydrogen / methanol / 14 h / 20 °C

6: triethylamine / dichloromethane / 1 h / 0 °C

With lithium borohydride; sodium azide; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 76387-70-7
(S)-3-amino-2-tert-butoxycarbonylaminopropionic acid

: 1429913-74-5
benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate; potassium hydroxide / tetrahydrofuran; water / 16 h / 0 - 20 °C

2: potassium carbonate / dimethyl sulfoxide / 12 h / 20 °C

3: lithium borohydride / tetrahydrofuran / 1 h / 0 - 20 °C

4: dichloromethane / 12 h / 0 - 20 °C

5: sodium azide / N,N-dimethyl-formamide / 24 h / 50 °C

6: palladium 10% on activated carbon; hydrogen / methanol / 14 h / 20 °C

7: triethylamine / dichloromethane / 1 h / 0 °C

With lithium borohydride; sodium azide; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1429913-70-1,1263045-28-8
benzyl tert-butyl (3-hydroxypropane-1,2-diyl)biscarbamate

: 1429913-74-5
benzyl tert-butyl[3-(acetylamino)propane-1,2-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: dichloromethane / 12 h / 0 - 20 °C

2: sodium azide / N,N-dimethyl-formamide / 24 h / 50 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 14 h / 20 °C

4: triethylamine / dichloromethane / 1 h / 0 °C

With sodium azide; palladium 10% on activated carbon; hydrogen; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;