C₂₄H₂₇ClN₂O₃S₂

Base Information

Chemical Name:C₂₄H₂₇ClN₂O₃S₂
CAS No.:1374354-48-9
Molecular Formula:C₂₄H₂₇ClN₂O₃S₂
Molecular Weight:491.075
Hs Code.:

C<sub>24</sub>H<sub>27</sub>ClN<sub>2</sub>O<sub>3</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₄H₂₇ClN₂O₃S₂

Chemical Property:

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Technology Process of C₂₄H₂₇ClN₂O₃S₂

There total 11 articles about C₂₄H₂₇ClN₂O₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₆ClNO₄SSi

: 1374354-48-9
C₂₄H₂₇ClN₂O₃S₂

Guidance literature:: Multi-step reaction with 4 steps

1: Lawessons reagent; pyridine / toluene / 100 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran

3: thionyl chloride / toluene

4: N-ethyl-N,N-diisopropylamine / acetonitrile

With Lawessons reagent; pyridine; thionyl chloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: C₁₁H₁₂BrClO₂

: 1374354-48-9
C₂₄H₂₇ClN₂O₃S₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium diformamide

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

3: Lawessons reagent; pyridine / toluene / 100 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran

5: thionyl chloride / toluene

6: N-ethyl-N,N-diisopropylamine / acetonitrile

With Lawessons reagent; pyridine; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067

Reference yield:

: 18791-75-8
4-Bromothiophen-2-aldehyde

: 1374354-48-9
C₂₄H₂₇ClN₂O₃S₂

Guidance literature:: Multi-step reaction with 9 steps

1: sodium tetrahydroborate / methanol

2: 1H-imidazole

3: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)

4: n-butyllithium / tetrahydrofuran

5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform

6: Lawessons reagent; pyridine / toluene / 100 °C

7: tetrabutyl ammonium fluoride / tetrahydrofuran

8: thionyl chloride / toluene

9: N-ethyl-N,N-diisopropylamine / acetonitrile

With Lawessons reagent; pyridine; 1H-imidazole; sodium tetrahydroborate; n-butyllithium; thionyl chloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); tetrabutyl ammonium fluoride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067