N,N'-bis(salicylidene)-1,2-phenylene-diaminocobalt(II)

Base Information

Chemical Name:N,N'-bis(salicylidene)-1,2-phenylene-diaminocobalt(II)
CAS No.:39836-45-8
Molecular Formula:C₂₀H₁₄CoN₂O₂
Molecular Weight:373.337
Hs Code.:

Synonyms:

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Chemical Property of N,N'-bis(salicylidene)-1,2-phenylene-diaminocobalt(II)

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Technology Process of N,N'-bis(salicylidene)-1,2-phenylene-diaminocobalt(II)

There total 2 articles about N,N'-bis(salicylidene)-1,2-phenylene-diaminocobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 90884-17-6
2,2′-((1,2-phenylenebis(azanediyl))bis(methylene))diphenol

: 39836-45-8
N,N'-(o-phenylene)bis(salicylideneiminato)cobalt(II)

Guidance literature:: With oxygen; In 1,4-dioxane; pyridine; Co salt and the diamine placed in a reactor heated at 60°C, mixt.of dioxan/pyridine (7/1) added, vessel filled with O2, heated under sti rring for ca. 80 min; ppt. sepd, dried in vac. at 100°C;
DOI:10.1023/A:1011389632581

Reference yield:

: 3946-91-6
N,N'-bis(salicylidene)-o-phenylenediamine

: 6147-53-1
cobalt(II) diacetate tetrahydrate

: 39836-45-8
N,N'-(o-phenylene)bis(salicylideneiminato)cobalt(II)

Guidance literature:: In propan-1-ol; soln. of Co(CH3COO)2*4H2O (0.016 mol) purged with N2 at stirring, warmedto 323 K under N2, H2salophen (0.016 mol) added, susp. stirred and heat ed under reflux (N2) for 8 h, cooled; A. Botther et al. Inorg. Chem. 32 (1993) 4131; filtered, ppt. washed with diethylether, dried in air, recrystd. from chloroform; elem. anal., detd. by XRD;
DOI:10.1016/j.ica.2009.07.023

Reference yield: 98.0%

: 17457-14-6,39836-45-8
N,N'-bis(salicylidene)-1,2-phenylene diaminocobalt(II)

: 201230-82-2
carbon monoxide

: 873-75-6
4-bromobenzenemethanol

: C₂₈H₂₀BrCoN₂O₄

Guidance literature:: With dipotassium peroxodisulfate; In 1,2-dichloro-ethane; at 20 ℃; for 48h; under 760.051 Torr; Darkness; Inert atmosphere;
DOI:10.1021/acs.organomet.7b00186