Diethyl 4-Acetamidobenzylphosphonate

Base Information

Chemical Name:Diethyl 4-Acetamidobenzylphosphonate
CAS No.:118578-84-0
Molecular Formula:C13H20NO4P
Molecular Weight:285.28
Hs Code.:
DSSTox Substance ID:DTXSID80432582
Nikkaji Number:J1.761.869E
Wikidata:Q82246656
Mol file:118578-84-0.mol

Synonyms:Diethyl 4-Acetamidobenzylphosphonate;118578-84-0;SCHEMBL1486740;DTXSID80432582;LSQQRLOYPDMBGI-UHFFFAOYSA-N;4-(Acetylamino)benzyldiethoxyphosphine oxide

Suppliers and Price of Diethyl 4-Acetamidobenzylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Diethyl 4-Acetamidobenzylphosphonate

Chemical Property:

XLogP3:0.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:285.11299512
Heavy Atom Count:19
Complexity:317

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(CC1=CC=C(C=C1)NC(=O)C)OCC

Technology Process of Diethyl 4-Acetamidobenzylphosphonate

There total 1 articles about Diethyl 4-Acetamidobenzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 20074-79-7
diethyl (4-aminobenzyl)phosphonate

: 108-24-7
acetic anhydride

: 118578-84-0
diethyl p-acetylaminobenzylphosphonate

Guidance literature:: for 2h; Ambient temperature;
DOI:10.1016/0223-5234(87)90039-0

Reference yield: 65.0%

: 118578-84-0
diethyl p-acetylaminobenzylphosphonate

: 73183-34-3
bis(pinacol)diborane

: 1374606-74-2
diethyl 4-acetamido-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzylphosphonate

Guidance literature:: With BQ; palladium diacetate; In acetic acid; 5 % Pd(OAc)2, 2 equiv (Bpin)2, 2 equiv BQ, 33%TsOH-AcOH, PfhCF3, 30°C;
DOI:10.1039/c2cc31737k