GeFS((C₃H₇)2C₆H₃)NCCH₃CHCCH₃N((C₃H₇)2C₆H₃)

Base Information

• Chemical Name: GeFS((C₃H₇)2C₆H₃)NCCH₃CHCCH₃N((C₃H₇)2C₆H₃)
• CAS No.: 452899-45-5
• Molecular Formula: C₂₉H₄₁FGeN₂S
• Molecular Weight: 541.312
• Mol file: 452899-45-5.mol

Synonyms:

Chemical Property of GeFS((C₃H₇)2C₆H₃)NCCH₃CHCCH₃N((C₃H₇)2C₆H₃)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of GeFS((C₃H₇)2C₆H₃)NCCH₃CHCCH₃N((C₃H₇)2C₆H₃)

There total 3 articles about GeFS((C₃H₇)2C₆H₃)NCCH₃CHCCH₃N((C₃H₇)2C₆H₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)Ge(S)Cl (452899-44-4) + trimethyltin fluoride (420-60-0) → GeFS((C3H7)2C6H3)NCCH3CHCCH3N((C3H7)2C6H3) (452899-45-5)

Guidance literature:

In dichloromethane; soln. of Ge-compound in CH2Cl2 was added to suspn. of Sn-compound in CH2Cl2, stirred for 2 d at room temp. under N2; volatiles were removed, extd. with toluene, stored at -32°C for 24 h; elem. anal.;

DOI:10.1039/b211617k

Reference yield: 71.0%

(((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)GeF (382150-85-8) + sulfur (7704-34-9) → GeFS((C3H7)2C6H3)NCCH3CHCCH3N((C3H7)2C6H3) (452899-45-5)

Guidance literature:

In toluene; soln. of Ge-compound in toluene was added to suspn. of S in toluene, stirred for 2 d under N2; filtered, stored at -32°C for 24 h;

DOI:10.1039/b211617k

Reference yield:

[C3H(CH3)2(N(2,6-diisopropylphenyl))2 chlorogermylene] (334719-93-6) → GeFS((C3H7)2C6H3)NCCH3CHCCH3N((C3H7)2C6H3) (452899-45-5)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: dichloromethane

In dichloromethane; toluene;

DOI:10.1039/b211617k

upstream raw materials:

(((CH₃)2CH)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)GeF

sulfur

(((CH₃)2CH)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)Ge(S)Cl

trimethyltin fluoride

Downstream raw materials:

L(Me)GeS