Technology Process of C36H36N4O7
There total 7 articles about C36H36N4O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
for 4h;
Inert atmosphere;
DOI:10.1039/c2cc36252j
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: N-benzyl-N,N,N-triethylammonium chloride; trichlorophosphate / N,N-dimethyl-aniline; acetonitrile / 1 h / 90 °C / Inert atmosphere
2.1: sodium hydride / acetonitrile; mineral oil / 1 h / 20 °C
2.2: 3.08 h
3.1: sodium hydroxide / water; 1,4-dioxane / 18 h / 90 °C
4.1: N,N-dimethyl-formamide / 1 h / Inert atmosphere
5.1: acetic acid / 20 °C
6.1: pyridine; dmap / 4 h / Inert atmosphere
With
pyridine; dmap; N-benzyl-N,N,N-triethylammonium chloride; sodium hydride; acetic acid; sodium hydroxide; trichlorophosphate;
In
1,4-dioxane; water; N,N-dimethyl-aniline; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1039/c2cc36252j
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: trichlorophosphate
2.1: sodium hydride / acetonitrile; mineral oil / 1 h / 20 °C
2.2: 3.08 h
3.1: sodium hydroxide / water; 1,4-dioxane / 18 h / 90 °C
4.1: N,N-dimethyl-formamide / 1 h / Inert atmosphere
5.1: acetic acid / 20 °C
6.1: pyridine; dmap / 4 h / Inert atmosphere
With
pyridine; dmap; sodium hydride; acetic acid; sodium hydroxide; trichlorophosphate;
In
1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1039/c2cc36252j