C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-)

Base Information

Chemical Name:C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-)
CAS No.:1448822-10-3
Molecular Formula:C₆₄H₆₅ClN₄O₆P*Cl
Molecular Weight:1088.12
Hs Code.:

C<sub>64</sub>H<sub>65</sub>ClN<sub>4</sub>O<sub>6</sub>P<sup>(1+)</sup>*Cl<sup>(1-)</sup>

Synonyms:

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Chemical Property of C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-)

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Technology Process of C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-)

There total 7 articles about C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1448822-25-0
C₄₆H₅₁ClN₄O₇

: 17814-85-6
(4-carboxybutyl)triphenylphosphonium bromide

: 1448822-10-3
C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-)

Guidance literature:: C₄₆H₅₁ClN₄O₇; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

(4-carboxybutyl)triphenylphosphonium bromide; With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; Further stages; Inert atmosphere;

Reference yield:

: 2513-23-7
2'-Carboxy-5-chloro-2,4-dihydroxybenzophenone

: 1448822-10-3
C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / 4 h / 100 °C / Sealed tube

2.1: triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20.5 h / 20 - 100 °C / Inert atmosphere; Schlenk technique

4.1: hydrogenchloride / water; acetic acid / 2 h / 100 °C

5.1: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

6.2: Inert atmosphere

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; water; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1448822-18-1
C₃₃H₃₁ClF₃NO₈S

: 1448822-10-3
C₆₄H₆₅ClN₄O₆P⁽¹⁺⁾*Cl^(1-)

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20.5 h / 20 - 100 °C / Inert atmosphere; Schlenk technique

2.1: hydrogenchloride / water; acetic acid / 2 h / 100 °C

3.1: triethylamine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

4.2: Inert atmosphere

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane; water; acetic acid; N,N-dimethyl-formamide; toluene;