(1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol

Base Information

Chemical Name:(1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol
CAS No.:1192482-00-0
Molecular Formula:C₃₁H₅₆O₅Si₂
Molecular Weight:564.954
Hs Code.:

(1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol

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Chemical Property of (1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol

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Technology Process of (1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol

There total 1 articles about (1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1192481-99-4
(3aR,4R,5R,6aS)-5-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}hexahydro-2H-cyclopenta[b]furan-2-one

: 1192482-00-0
(1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol

Guidance literature:: With lithium borohydride; In tetrahydrofuran; at 0 - 35 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo901497u

Reference yield:

: 1192482-00-0
(1S,2R,3S,4R)-4-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-3-{(1E,3S)-3-{[dimethyl(2-methyl-2-propanyl)silyl]oxy}-4-[3-(methoxymethyl)phenyl]-1-buten-1-yl}-2-(2-hydroxyethyl)cyclopentanol

: 124-63-0
methanesulfonyl chloride

: C₃₂H₅₈O₇SSi₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; at -20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo901497u