4-(But-3-enyloxy)phenol

Base Information

Chemical Name:4-(But-3-enyloxy)phenol
CAS No.:118909-86-7
Molecular Formula:C10H12O2
Molecular Weight:164.204
Hs Code.:
DSSTox Substance ID:DTXSID60708171
Nikkaji Number:J1.390.095G
Wikidata:Q82642314
Mol file:118909-86-7.mol

Synonyms:4-But-3-enoxyphenol;4-(but-3-enyloxy)phenol;118909-86-7;Phenol, 4-(3-butenyloxy)-;4-(3-butenyloxy)phenol;4-allylmethoxyphenol;SCHEMBL5850328;DTXSID60708171;BKQYNWJOMDZBMG-UHFFFAOYSA-N;4-[(But-3-en-1-yl)oxy]phenol;AKOS013635475;A1-06229

Suppliers and Price of 4-(But-3-enyloxy)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-(But-3-enyloxy)phenol

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:164.083729621
Heavy Atom Count:12
Complexity:126

Purity/Quality:: 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCCOC1=CC=C(C=C1)O

Technology Process of 4-(But-3-enyloxy)phenol

There total 5 articles about 4-(But-3-enyloxy)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 5162-44-7
1-bromo-4-butene

: 123-31-9,8027-02-9
hydroquinone

: 118909-86-7
4-(but-3-en-1-yloxy)phenol

Guidance literature:: With potassium carbonate; In acetonitrile; for 12h; Reflux;
DOI:10.1021/jo900012z

Reference yield:

: 2444-19-1
4-hydroxyphenyl benzoate

: 118909-86-7
4-(but-3-en-1-yloxy)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 7 h / 20 °C / Inert atmosphere

2.1: potassium hydroxide / ethanol / 3 h / Reflux

With triphenylphosphine; potassium hydroxide; In tetrahydrofuran; ethanol; 1.1: Mitsunobu reaction / 1.2: Mitsunobu reaction;
DOI:10.1039/c0jm03691a

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 118909-86-7
4-(but-3-en-1-yloxy)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / water / 20 h / 20 °C / Inert atmosphere

2.1: triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 7 h / 20 °C / Inert atmosphere

3.1: potassium hydroxide / ethanol / 3 h / Reflux

With potassium carbonate; triphenylphosphine; potassium hydroxide; In tetrahydrofuran; ethanol; water; 2.1: Mitsunobu reaction / 2.2: Mitsunobu reaction;
DOI:10.1039/c0jm03691a