1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl

Base Information

Chemical Name:1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl
CAS No.:1252007-18-3
Molecular Formula:C₄₇H₇₂P₂S
Molecular Weight:731.102
Hs Code.:

Synonyms:

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Chemical Property of 1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl

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Technology Process of 1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl

There total 1 articles about 1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 594-19-4
tert.-butyl lithium

: 100938-86-1
2-(2,4,6-tri-tert-butylphenyl)phosphaacetylene

: 1252007-18-3
1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl

Guidance literature:: tert.-butyl lithium; 2-(2,4,6-tri-tert-butylphenyl)phosphaacetylene; In tetrahydrofuran; diethyl ether; cyclohexane; at -78 - 20 ℃; for 1.16667h; Inert atmosphere;

3-thienylmethyl halide; In tetrahydrofuran; diethyl ether; cyclohexane; for 1h; Inert atmosphere;
DOI:10.1039/c0dt00532k

Reference yield:

: 1252007-18-3
1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl

: C₄₂H₆₇P₂^(1-)*Li⁽¹⁺⁾

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1h; regioselective reaction;
DOI:10.1039/c0dt00532k

Reference yield:

: 1252007-18-3
1-t-butyl-3-(3-thienyl)methyl-2,4-bis(2,4,6-tri-t-butylphenyl)-1,3-diphosphacyclobutane-2,4-diyl

: 1182842-83-6
C₄₃H₇₂P₂

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 20 °C

2: tetrahydrofuran

3: lithium aluminium tetrahydride

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1039/c0dt00532k