azalactone of N-benzoyl-p-difluoromethoxyphenylalanine

Base Information

• Chemical Name: azalactone of N-benzoyl-p-difluoromethoxyphenylalanine
• CAS No.: 122749-01-3
• Molecular Formula: C₁₇H₁₃F₂NO₃
• Molecular Weight: 317.292
• Mol file: 122749-01-3.mol

Synonyms:

Chemical Property of azalactone of N-benzoyl-p-difluoromethoxyphenylalanine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of azalactone of N-benzoyl-p-difluoromethoxyphenylalanine

There total 1 articles about azalactone of N-benzoyl-p-difluoromethoxyphenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

azalactone of N-benzoyl-p-difluoromethoxy-α-aminocinnamic acid (122748-95-2) → azalactone of N-benzoyl-p-difluoromethoxyphenylalanine (122749-01-3)

Guidance literature:

With hydrogen; triethylamine; palladium dichloride; In 1,2-dimethoxyethane;

DOI:10.1007/BF00953628

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + azalactone of N-benzoyl-p-difluoromethoxyphenylalanine (122749-01-3) → S,S-(-)-α-phenylethylamide of N-benzoyl-p-difluoromethoxyphenylalanine (122748-97-4)

Guidance literature:

In 1,2-dimethoxyethane; for 12h; Yield given;

DOI:10.1007/BF00953628

upstream raw materials:

azalactone of N-benzoyl-p-difluoromethoxy-α-aminocinnamic acid

Downstream raw materials:

S,S-(-)-α-phenylethylamide of N-benzoyl-p-difluoromethoxyphenylalanine