Ethyl 2-(3,5-dichlorophenoxy)acetate

Base Information

Chemical Name:Ethyl 2-(3,5-dichlorophenoxy)acetate
CAS No.:119024-29-2
Molecular Formula:C10H10Cl2O3
Molecular Weight:249.094
Hs Code.:
DSSTox Substance ID:DTXSID60655994
Wikidata:Q82570425
Mol file:119024-29-2.mol

Synonyms:119024-29-2;Ethyl 2-(3,5-dichlorophenoxy)acetate;Ethyl 2-(3,5-dichloro-phenoxy)acetate;SCHEMBL5360710;DTXSID60655994;Ethyl (3,5-dichlorophenoxy)acetate;Ethyl2-(3,5-dichlorophenoxy)acetate;AKOS008952620

Suppliers and Price of Ethyl 2-(3,5-dichlorophenoxy)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Ethyl 2-(3,5-dichlorophenoxy)acetate

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:248.0006996
Heavy Atom Count:15
Complexity:201

Purity/Quality:: 95%-98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)COC1=CC(=CC(=C1)Cl)Cl

Technology Process of Ethyl 2-(3,5-dichlorophenoxy)acetate

There total 1 articles about Ethyl 2-(3,5-dichlorophenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-35-5
3,5-dichlorophenol

: 105-36-2
ethyl bromoacetate

: 119024-29-2
ethyl 2-(3,5-dichlorophenoxy)acetate

Guidance literature:: 3,5-dichlorophenol; With sodium; In acetone; at 20 ℃;

ethyl bromoacetate; In acetone; Reflux;
DOI:10.1021/jf062562t

Reference yield: 68.0%

: 119024-29-2
ethyl 2-(3,5-dichlorophenoxy)acetate

: 2-(3,5-dichlorophenoxy)acetohydroxamic acid

Guidance literature:: With hydroxylamine hydrochloride; sodium methylate; In methanol; at 20 ℃;
DOI:10.1016/j.bmc.2018.07.003

Reference yield:

: 119024-29-2
ethyl 2-(3,5-dichlorophenoxy)acetate

: 1226145-00-1
ethyl 4-(3,5-dichlorophenoxy)-3-oxobutanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / water / 4 h / 90 °C

2.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

4.2: 8 h / -78 °C

With oxalyl dichloride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm2014277