N-Benzyl-4-MethoxybenzenesulfonaMide, 97%

Base Information

• Chemical Name: N-Benzyl-4-MethoxybenzenesulfonaMide, 97%
• CAS No.: 119059-70-0
• Molecular Formula: C14H15NO3S
• Molecular Weight: 277.344
• Mol file: 119059-70-0.mol

Synonyms:N-benzyl-p-methoxybenzenesulfonamide;N-Benzyl-4-methoxy-benzenesulfonamide;N-benzyl-4-methoxyphenylsulfonamide;N-Benzyl p-methoxybenzenesulfonamide;N-benzyl 4-methoxyphenyl-sulphonamide;N-[4-methoxybenzenesulfonyl]-benzylamine;

Chemical Property of N-Benzyl-4-MethoxybenzenesulfonaMide, 97%

Chemical Property:

• Melting Point: 108-109 °C
• Boiling Point: 442.3±55.0 °C(Predicted)
• PKA: 11.74±0.30(Predicted)
• PSA: 63.78000
• Density: 1.234±0.06 g/cm3(Predicted)
• LogP: 3.64540

Purity/Quality:

99% ^*data from raw suppliers

N-Benzyl-4-methoxybenzenesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Benzyl-4-MethoxybenzenesulfonaMide, 97%

There total 21 articles about N-Benzyl-4-MethoxybenzenesulfonaMide, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-benzylidene-4-methoxy-benzenesulfonamide (52960-60-8) → N-benzyl-4-methoxybenzenesulfonamide (119059-70-0)

Guidance literature:

With Schwartz's reagent; In dichloromethane; at 20 ℃; for 0.333333h; chemoselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejoc.201901607

Reference yield: 99.0%

4-methoxybenzene sulfonamide (1129-26-6) + benzyl alcohol (100-51-6,185532-71-2) → N-benzyl-4-methoxybenzenesulfonamide (119059-70-0)

Guidance literature:

With Wilkinson's catalyst; potassium carbonate; at 120 ℃; for 12h; Sealed tube;

DOI:10.1016/j.cclet.2011.03.014

Reference yield: 97.0%

4-methoxy-phenyl-sulphonyl chloride (98-68-0) + benzylamine (100-46-9) → N-benzyl-4-methoxybenzenesulfonamide (119059-70-0)

Guidance literature:

With triethylamine; In chloroform; 1.) RT, 1 h, 2.) reflux, 1 h;

DOI:10.1021/jm960871c

upstream raw materials:

4-methoxy-phenyl-sulphonyl chloride

benzylamine

2,4-dinitrophenyl 4-methoxybenzenesulfonate

toluene

Downstream raw materials:

C₁₉H₂₃NO₅S

ethyl 2-[[4-methoxybenzenesulfonyl](benzyl)amino]acetate

N-Benzyl-N-(2-cyano-6-trifluoromethyl-phenyl)-4-methoxy-benzenesulfonamide

4-[benzyl-(4-methoxy-benzenesulfonyl)-amino]-8-methyl-quinoline-3-carboxylic acid ethyl ester