[(N,N'-bis(2-(dimethylamino)athyl)dibenzofuran-4,6-diamine^(2-))Zn₂Ph₂]

Base Information

• Chemical Name: [(N,N'-bis(2-(dimethylamino)athyl)dibenzofuran-4,6-diamine^(2-))Zn₂Ph₂]
• CAS No.: 864362-87-8
• Molecular Formula: C₃₂H₃₆N₄OZn₂
• Molecular Weight: 623.444

Synonyms:

Chemical Property of [(N,N'-bis(2-(dimethylamino)athyl)dibenzofuran-4,6-diamine^(2-))Zn₂Ph₂]

Chemical Property:

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Technology Process of [(N,N'-bis(2-(dimethylamino)athyl)dibenzofuran-4,6-diamine^(2-))Zn₂Ph₂]

There total 1 articles about [(N,N'-bis(2-(dimethylamino)athyl)dibenzofuran-4,6-diamine^(2-))Zn₂Ph₂] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.3%

diphenylzinc (1078-58-6) + N,N'-bis(2-(dimethylamino)ethyl)dibenzofuran-4,6-diamine → [(N,N'-bis(2-(dimethylamino)athyl)dibenzofuran-4,6-diamine(2-))Zn2Ph2] (864362-87-8,869541-63-9)

Guidance literature:

In toluene; react. ZnPh2 and ligand in toluene at 75°C for 1 h; soln. was filtered warm and cooled to -15°C overnight, ppt. was filtered and dried in vacuo; elem. anal.;

DOI:10.1021/om050580e

Reference yield: 86.7%

[(N,N'-bis(2-(dimethylamino)athyl)dibenzofuran-4,6-diamine(2-))Zn2Ph2] (864362-87-8,869541-63-9) + benzaldehyde (100-52-7) → [(N,N'-bis(2-(dimethylamino)ethyl)dibenzofuran-4,6-diamine(2-))Zn2(Ph)(OCHPh2)] (869541-65-1)

Guidance literature:

In benzene; react. Zn complex and benzaldehyde (1:1) in benzene for 24 h; ppt. was recrystd. by hexane vapor diffusion into CH2Cl2 soln.; elem. anal.;

DOI:10.1021/om050580e

Reference yield: 76.0%

Trimethylphosphine oxide (676-96-0) + [Zn2(C6H5)2(C12H6O(NCH2CH2N(CH3)2)2)] (864362-87-8,869541-63-9) + toluene (108-88-3,15644-74-3,16713-13-6) → [Zn2(C12H6O(NCH2CH2N(CH3)2)2)(C6H5)2(OP(CH3)3)2]*0.5C6H5CH3

Guidance literature:

In toluene; Me3PO (2 equiv.) added to warm soln. of Zn complex in toluene; cooled to ambient temp.;

DOI:10.1021/om050474c

upstream raw materials:

diphenylzinc

Downstream raw materials:

[(N,N'-bis(2-(dimethylamino)ethyl)dibenzofuran-4,6-diamine^(2-))Zn₂(Ph)(OCHPh₂)]

[(N,N'-bis(2-(dimethylamino)ethyl)dibenzofuran-4,6-diamine^(2-))Zn₂(OCHPh₂)2]

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