trans-1,2-dibenzoylcyclohexane

Base Information

Chemical Name:trans-1,2-dibenzoylcyclohexane
CAS No.:104722-26-1
Molecular Formula:C₂₀H₂₀O₂
Molecular Weight:292.378
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-1,2-dibenzoylcyclohexane

Chemical Property:

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Technology Process of trans-1,2-dibenzoylcyclohexane

There total 4 articles about trans-1,2-dibenzoylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 2305-32-0
trans-1,2-cyclohexanedicarboxylic acid

: 591-51-5
phenyllithium

: 104722-26-1
trans-1,2-dibenzoylcyclohexane

Guidance literature:: In tetrahydrofuran; diethyl ether; for 16h; Ambient temperature;
DOI:10.1246/bcsj.58.3118

Reference yield:

: 6268-58-2
1,8-diphenyl-1,8-octanedione

: 1382963-93-0
cis-1,2-dibenzoylcyclohexane

: 104722-26-1
trans-1,2-dibenzoylcyclohexane

Guidance literature:: 1,8-diphenyl-1,8-octanedione; With zinc(II) chloride; lithium diisopropyl amide;

With copper acetylacetonate; oxygen; In tetrahydrofuran; at 20 ℃; for 0.166667h; Overall yield = 55 %;
DOI:10.1021/om300393m

Reference yield:

: 2305-32-0
trans-1,2-cyclohexanedicarboxylic acid

: 104722-26-1
trans-1,2-dibenzoylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus (V)-chloride

2: AlCl₃; carbon disulfide

With carbon disulfide; aluminium trichloride; phosphorus pentachloride;
DOI:10.1021/jo01177a010