C₅₃H₈₂O₈Si₂

Base Information

• Chemical Name: C₅₃H₈₂O₈Si₂
• CAS No.: 1283736-14-0
• Molecular Formula: C₅₃H₈₂O₈Si₂
• Molecular Weight: 903.4
• Mol file: 1283736-14-0.mol

Synonyms:

Chemical Property of C₅₃H₈₂O₈Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₃H₈₂O₈Si₂

There total 20 articles about C₅₃H₈₂O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C56H88O7S2Si2 (1283735-98-7) → C53H82O8Si2 (1283736-14-0)

Guidance literature:

With bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate; In dichloromethane; water; acetonitrile; at 0 ℃; for 0.166667h;

DOI:10.1002/asia.201000882

Reference yield:

C28H36O4Si (1202748-08-0) → C53H82O8Si2 (1283736-14-0)

Guidance literature:

Multi-step reaction with 6 steps

1.1: ammonium cerium (IV) nitrate; sodium hydrogencarbonate / water; acetonitrile / 0.17 h / 0 °C

2.1: 1H-imidazole; dmap / 0 - 20 °C

3.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 6 h / 0 °C

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C

5.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

5.2: -78 - 20 °C

6.1: bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate / dichloromethane; water; acetonitrile / 0.17 h / 0 °C

With 1H-imidazole; dmap; n-butyllithium; ammonium cerium (IV) nitrate; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;

DOI:10.1002/asia.201000882

Reference yield:

C21H30O3Si (1202747-69-0) → C53H82O8Si2 (1283736-14-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: 1H-imidazole; dmap / 0 - 20 °C

2.1: pyridinium p-toluenesulfonate / methanol; dichloromethane / 6 h / 0 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C

4.1: n-butyllithium / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.2: -78 - 20 °C

5.1: bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate / dichloromethane; water; acetonitrile / 0.17 h / 0 °C

With 1H-imidazole; dmap; n-butyllithium; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; bis-[(trifluoroacetoxy)iodo]benzene; calcium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;

DOI:10.1002/asia.201000882

upstream raw materials:

C₂₈H₃₆O₄Si

C₂₁H₃₀O₃Si

C₂₂H₃₄O₄

C₂₆H₄₂O₆

Downstream raw materials:

C₅₅H₈₆O₁₁Si₂

C₅₅H₈₆O₁₁Si₂

C₅₅H₈₄O₉Si₂