6-Benzyloxy-5-methoxy-1,4-naphthochinon

Base Information

Chemical Name:6-Benzyloxy-5-methoxy-1,4-naphthochinon
CAS No.:99316-59-3
Molecular Formula:C₁₈H₁₄O₄
Molecular Weight:294.307
Hs Code.:

Synonyms:

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Chemical Property of 6-Benzyloxy-5-methoxy-1,4-naphthochinon

Chemical Property:

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Technology Process of 6-Benzyloxy-5-methoxy-1,4-naphthochinon

There total 10 articles about 6-Benzyloxy-5-methoxy-1,4-naphthochinon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75445-61-3
5-(benzyloxy)-1,4-dihydronaphthalene-1,4-dione

: 99316-59-3
6-Benzyloxy-5-methoxy-1,4-naphthochinon

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid, Zn / CHCl₃; methanol

2: NaOH / dioxane; H₂O / 1.) room temp.; 2.) 45 deg C, 10 min

3: sodium acetate, H₂ / Pd/C (10percent Pd) / benzene; methanol / 40 °C / 760 Torr

4: 74 percent / KH₂PO₄, Fremy-salt, 1 N NaOH / H₂O; acetone; ethanol / 0.25 h

5: AlCl₃

6: 43 percent / AgO / CHCl₃

7: AgO / CHCl₃ / Ambient temperature

With silver(II) oxide; sodium hydroxide; potassium dihydrogenphosphate; aluminium trichloride; potassium nitrososulfonate; hydrogen; sodium acetate; acetic acid; zinc; 10% palladium on active carbon; In 1,4-dioxane; methanol; ethanol; chloroform; water; acetone; benzene;

Reference yield:

: 75445-68-0
5-Benzyloxy-naphthalene-1,4-diol

: 99316-59-3
6-Benzyloxy-5-methoxy-1,4-naphthochinon

Guidance literature:: Multi-step reaction with 6 steps

1: NaOH / dioxane; H₂O / 1.) room temp.; 2.) 45 deg C, 10 min

2: sodium acetate, H₂ / Pd/C (10percent Pd) / benzene; methanol / 40 °C / 760 Torr

3: 74 percent / KH₂PO₄, Fremy-salt, 1 N NaOH / H₂O; acetone; ethanol / 0.25 h

4: AlCl₃

5: 43 percent / AgO / CHCl₃

6: AgO / CHCl₃ / Ambient temperature

With silver(II) oxide; sodium hydroxide; potassium dihydrogenphosphate; aluminium trichloride; potassium nitrososulfonate; hydrogen; sodium acetate; 10% palladium on active carbon; In 1,4-dioxane; methanol; ethanol; chloroform; water; acetone; benzene;

Reference yield:

: 89474-91-9
1-Benzyloxy-4-chlor-5,8-dimethoxynaphthalin

: 99316-59-3
6-Benzyloxy-5-methoxy-1,4-naphthochinon

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / sodium acetate, H₂ / Pd/C (10percent Pd) / benzene; methanol / 40 °C / 760 Torr

2: 74 percent / KH₂PO₄, Fremy-salt, 1 N NaOH / H₂O; acetone; ethanol / 0.25 h

3: AlCl₃

4: 43 percent / AgO / CHCl₃

5: AgO / CHCl₃ / Ambient temperature

With silver(II) oxide; sodium hydroxide; potassium dihydrogenphosphate; aluminium trichloride; potassium nitrososulfonate; hydrogen; sodium acetate; 10% palladium on active carbon; In methanol; ethanol; chloroform; water; acetone; benzene;