Technology Process of 1-(2-Isopropoxy-5-methoxyphenyl)-1H-1,2,3-triazolo<4,5-c>pyridine
There total 6 articles about 1-(2-Isopropoxy-5-methoxyphenyl)-1H-1,2,3-triazolo<4,5-c>pyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; sodium nitrite;
In
water;
1) 0 deg C, 10 min, 2) r.t., 30 min;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94 percent / H2 / 10percent Pd/C / methanol / 5 h / 26 °C / 760 Torr
2: 72 percent / NaOAc, gl. AcOH / Heating
3: 59 percent / H2 / 10percent Pd/C / methanol / 760 Torr / Ambient temperature
4: 71 percent / NaNO2, 0.1N aq. HCl / H2O / 1) 0 deg C, 10 min, 2) r.t., 30 min
With
hydrogenchloride; hydrogen; sodium acetate; acetic acid; sodium nitrite;
palladium on activated charcoal;
In
methanol; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 72 percent / conc. HNO3 (d=1.42), propionic acid, gl. AcOH / 0.42 h / 0 °C
2: 94 percent / H2 / 10percent Pd/C / methanol / 5 h / 26 °C / 760 Torr
3: 72 percent / NaOAc, gl. AcOH / Heating
4: 59 percent / H2 / 10percent Pd/C / methanol / 760 Torr / Ambient temperature
5: 71 percent / NaNO2, 0.1N aq. HCl / H2O / 1) 0 deg C, 10 min, 2) r.t., 30 min
With
hydrogenchloride; hydrogen; nitric acid; sodium acetate; acetic acid; propionic acid; sodium nitrite;
palladium on activated charcoal;
In
methanol; water;
