tetrachlorobis(salicylaldehyde-N'-pyridyl sulphanilamide)germanium

Base Information

Chemical Name:tetrachlorobis(salicylaldehyde-N'-pyridyl sulphanilamide)germanium
CAS No.:101996-04-7
Molecular Formula:C₃₆H₃₀Cl₄GeN₆O₆S₂
Molecular Weight:921.205
Hs Code.:

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Chemical Property of tetrachlorobis(salicylaldehyde-N'-pyridyl sulphanilamide)germanium

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Technology Process of tetrachlorobis(salicylaldehyde-N'-pyridyl sulphanilamide)germanium

There total 1 articles about tetrachlorobis(salicylaldehyde-N'-pyridyl sulphanilamide)germanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 95107-48-5
salicylaldehyde sulfapyridine

: 10038-98-9
germaniumtetrachloride

: 101996-04-7
tetrachlorobis(salicylaldehyde-N'-pyridyl sulphanilamide)germanium

Guidance literature:: In benzene; to a soln. of GeCl4 in benzene the ligand in 1:2 molar ratio was added,the mixt. was stirred for 3-4 h, the product sepd. slowly; the solvent was decanted off, the solid was washed with benzene, the solvent was removed in vac., dried at 40-50°C 0.05 mm for 2-3 h; elem. anal.;