Benzenesulfonamide, 4-[[(2-hydroxyphenyl)methylene]amino]-N-2-pyridinyl-

Base Information

Chemical Name:Benzenesulfonamide, 4-[[(2-hydroxyphenyl)methylene]amino]-N-2-pyridinyl-
CAS No.:95107-48-5
Molecular Formula:C18H15N3O3S
Molecular Weight:353.401
Hs Code.:

Synonyms:

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Chemical Property of Benzenesulfonamide, 4-[[(2-hydroxyphenyl)methylene]amino]-N-2-pyridinyl-

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Technology Process of Benzenesulfonamide, 4-[[(2-hydroxyphenyl)methylene]amino]-N-2-pyridinyl-

There total 1 articles about Benzenesulfonamide, 4-[[(2-hydroxyphenyl)methylene]amino]-N-2-pyridinyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 144-83-2
sulphapyridine

: 90-02-8
salicylaldehyde

: 95107-48-5
N-salicylidene-sulfanilic acid-[2]pyridylamide

Guidance literature:: With sodium acetate; acetic acid; In ethanol; for 4h; Heating;

Reference yield: 90.0%

: 95107-48-5
salicylaldehyde sulfapyridine

: 10038-98-9
germaniumtetrachloride

: 101996-04-7
tetrachlorobis(salicylaldehyde-N'-pyridyl sulphanilamide)germanium

Guidance literature:: In benzene; to a soln. of GeCl4 in benzene the ligand in 1:2 molar ratio was added,the mixt. was stirred for 3-4 h, the product sepd. slowly; the solvent was decanted off, the solid was washed with benzene, the solvent was removed in vac., dried at 40-50°C 0.05 mm for 2-3 h; elem. anal.;

Reference yield: 80.0%

: 95107-48-5
salicylaldehyde sulfapyridine

: 2-isopropoxy-1,3,2-dithioborole

: SC₆H₄SBOC₆H₄CHNC₆H₄SO₂NHC₅H₄N

Guidance literature:: In benzene; byproducts: i-PrOH; The mixt. of boron compound and azomethine (1:1 molar ratio) in dry benzene was refluxed for 10 h;; solvents was removed, washed with dry n-hexane, dried under vac.; elem.anal.;;