{(S)-1-[(S)-1-{(1S,2S)-3-[(S)-1-(3-Aminomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-1-cyclohexylmethyl-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

Base Information

• Chemical Name: {(S)-1-[(S)-1-{(1S,2S)-3-[(S)-1-(3-Aminomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-1-cyclohexylmethyl-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester
• CAS No.: 100902-07-6
• Molecular Formula: C₄₅H₆₆N₈O₇
• Molecular Weight: 831.068

Synonyms:

Chemical Property of {(S)-1-[(S)-1-{(1S,2S)-3-[(S)-1-(3-Aminomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-1-cyclohexylmethyl-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

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Technology Process of {(S)-1-[(S)-1-{(1S,2S)-3-[(S)-1-(3-Aminomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-1-cyclohexylmethyl-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

There total 1 articles about {(S)-1-[(S)-1-{(1S,2S)-3-[(S)-1-(3-Aminomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-1-cyclohexylmethyl-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-di(aminomethyl)benzene (1477-55-0) + Boc-L-Phe-L-His-(3S,4S)-ACHPA-L-Leu-OCH3 (115464-34-1) → {(S)-1-[(S)-1-{(1S,2S)-3-[(S)-1-(3-Aminomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-1-cyclohexylmethyl-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester (100902-07-6)

Guidance literature:

Multistep reaction;

DOI:10.1021/jm00118a009

Reference yield:

3,5-dimethyl-1-pyrazolylformaminidium nitrate (38184-47-3) + {(S)-1-[(S)-1-{(1S,2S)-3-[(S)-1-(3-Aminomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-1-cyclohexylmethyl-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester (100902-07-6) → {(S)-1-[(S)-1-{(1S,2S)-1-Cyclohexylmethyl-3-[(S)-1-(3-guanidinomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester (100902-08-7)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1021/jm00118a009

upstream raw materials:

1,3-di(aminomethyl)benzene

Boc-L-Phe-L-His-(3S,4S)-ACHPA-L-Leu-OCH₃

Downstream raw materials:

{(S)-1-[(S)-1-{(1S,2S)-1-Cyclohexylmethyl-3-[(S)-1-(3-guanidinomethyl-benzylcarbamoyl)-3-methyl-butylcarbamoyl]-2-hydroxy-propylcarbamoyl}-2-(3H-imidazol-4-yl)-ethylcarbamoyl]-2-phenyl-ethyl}-carbamic acid tert-butyl ester

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