[(C6H4(CH2OCH3)(CH2P(C(CH3)3)2))PdCl(μ-Cl)]2

Base Information

Chemical Name:[(C6H4(CH2OCH3)(CH2P(C(CH3)3)2))PdCl(μ-Cl)]2
CAS No.:1277173-51-9
Molecular Formula:C₃₄H₅₈Cl₄O₂P₂Pd₂
Molecular Weight:915.433
Hs Code.:

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Chemical Property of [(C6H4(CH2OCH3)(CH2P(C(CH3)3)2))PdCl(μ-Cl)]2

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Technology Process of [(C6H4(CH2OCH3)(CH2P(C(CH3)3)2))PdCl(μ-Cl)]2

There total 2 articles about [(C6H4(CH2OCH3)(CH2P(C(CH3)3)2))PdCl(μ-Cl)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.7%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 1277173-50-8
C₆H₄(CH₂OCH₃)(CH₂P(C(CH₃)3)2)

: 1277173-51-9
[(C6H4(CH2OCH3)(CH2P(C(CH3)3)2))PdCl(μ-Cl)]2

Guidance literature:: In toluene; byproducts: C6H5CN; under N2 atm.; to ligand and Pd complex added toluene; soln. heated to 100°C; stirred for 4 h; cooled to room temp. over 12 h; solid isolated; rinsed (cold pentane); dried (vac.) for 12 h;
DOI:10.1021/om101150y

Reference yield:

: 7647-01-0,15364-23-5
hydrogenchloride

: 1277173-52-0
(C₆H₃(CH₂OCH₃)(CH₂P(C(CH₃)3)2))PdCl

: 1277173-51-9
[(C6H4(CH2OCH3)(CH2P(C(CH3)3)2))PdCl(μ-Cl)]2

Guidance literature:: In benzene-d6; under N2 atm.; HCl added to soln. of Pd complex in C6D6; not isolated; monitored by NMR spectroscopy;
DOI:10.1021/om101150y