ClRh(C₂F₄)(P(C₆H₅)3)2

Base Information

• Chemical Name: ClRh(C₂F₄)(P(C₆H₅)3)2
• CAS No.: 12216-72-7
• Molecular Formula: C₃₈H₃₀ClF₄P₂Rh
• Molecular Weight: 762.956

Synonyms:

Chemical Property of ClRh(C₂F₄)(P(C₆H₅)3)2

Chemical Property:

Purity/Quality:

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Technology Process of ClRh(C₂F₄)(P(C₆H₅)3)2

There total 1 articles about ClRh(C₂F₄)(P(C₆H₅)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{ClRh(η2-C2H4)(η2-C2F4)}2 → ClRh(C2F4)(P(C6H5)3)2 (12216-72-7,33009-49-3)

Guidance literature:

With triphenyl phosphine; In dichloromethane; The soln. of complex in THF was treated with a soln. of PPh3 in CH2Cl2 dropwise with stirring over 1 h and was stirred for 14 h ( atm. N2);; volume was reduced, pentane was added, ppt. was isolated;;

DOI:10.1021/om00148a016

Reference yield:

ClRh(C2F4)(P(C6H5)3)2 (12216-72-7,33009-49-3) + tris(dimethylamino)sulfonium trimethylsilyldifluoride (150746-76-2) → FRh(C2F4)(P(C6H5)3)2 (107272-42-4)

Guidance literature:

With AgBF₄; In tetrahydrofuran; byproducts: AgCl; Soln. of complex and AgBF4 in THF was stirred for 1 h at room temp.; filtered and was treated with 2 equiv of (Me2N)3S(1+)*Me3SiF2(1-); soln. was stirred for 1 h (atm. N2);; cooling to -35°C for 12 h; recrystd. from CH2Cl2/ether/pentane; elem. anal.;;

DOI:10.1021/om00148a016

Downstream raw materials:

FRh(C₂F₄)(P(C₆H₅)3)2

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