(1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether

Base Information

Chemical Name:(1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether
CAS No.:138944-97-5
Molecular Formula:C₁₅H₂₆O₃
Molecular Weight:254.37
Hs Code.:

Synonyms:

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Chemical Property of (1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether

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Technology Process of (1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether

There total 4 articles about (1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 138944-97-5,138945-35-4
(1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.02 g / pyridinium p-toluenesulfonate / CH₂Cl₂ / 7 h / Ambient temperature

2: 1) borane-THF complex, 2) 35percent H₂O₂, 3N KOH / 1) THF, -65 deg C, 2) 65 deg C, 15 h

With potassium hydroxide; borane-THF; dihydrogen peroxide; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1248/cpb.39.2514

Reference yield:

: 76339-71-4
(2S,3R,5S)-2-methyl-5-(1-methylethenyl)-3-(phenylseleno)-cyclohexanone

: 138944-97-5,138945-35-4
(1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 78.5 percent / LiAlH₄ / diethyl ether / 0.08 h / 0 °C

2: 1.02 g / pyridinium p-toluenesulfonate / CH₂Cl₂ / 7 h / Ambient temperature

3: 1) borane-THF complex, 2) 35percent H₂O₂, 3N KOH / 1) THF, -65 deg C, 2) 65 deg C, 15 h

With potassium hydroxide; lithium aluminium tetrahydride; borane-THF; dihydrogen peroxide; pyridinium p-toluenesulfonate; In diethyl ether; dichloromethane;
DOI:10.1248/cpb.39.2514

Reference yield:

: 90056-25-0
(1S,2S,3R,5S)-2-methyl-5-(1-methylethenyl)-3-(phenylseleno)-cyclohexanol

: 138944-97-5,138945-35-4
(1S,2R,5S)-5-(1-hydroxypropan-2-yl)-2-methyl-3-cyclohexenol tetrahydropyranyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 1.02 g / pyridinium p-toluenesulfonate / CH₂Cl₂ / 7 h / Ambient temperature

2: 1) borane-THF complex, 2) 35percent H₂O₂, 3N KOH / 1) THF, -65 deg C, 2) 65 deg C, 15 h

With potassium hydroxide; borane-THF; dihydrogen peroxide; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1248/cpb.39.2514