Technology Process of C17H14N4O7
There total 7 articles about C17H14N4O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / 22 h / Reflux
2: water; sodium hydroxide / 1,4-dioxane; ethanol / 0.58 h / 20 °C
3: thionyl chloride / chloroform / 1 h / Reflux
4: tetrahydrofuran; diethyl ether / 1.17 h / 0 - 20 °C / Inert atmosphere
With
thionyl chloride; water; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; chloroform; acetone;
DOI:10.1002/chem.201102732
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride / chloroform / 1 h / Reflux
2: tetrahydrofuran; diethyl ether / 1.17 h / 0 - 20 °C / Inert atmosphere
With
thionyl chloride;
In
tetrahydrofuran; diethyl ether; chloroform;
DOI:10.1002/chem.201102732
- Guidance literature:
-
Multi-step reaction with 7 steps
1: nitric acid; acetic acid / diethyl ether; water / 4.42 h / Cooling with ice
2: potassium tert-butylate / N,N-dimethyl-formamide / 1.33 h
3: sulfuric acid / 17 h / 0 °C / Reflux
4: potassium carbonate / acetone / 22 h / Reflux
5: water; sodium hydroxide / 1,4-dioxane; ethanol / 0.58 h / 20 °C
6: thionyl chloride / chloroform / 1 h / Reflux
7: tetrahydrofuran; diethyl ether / 1.17 h / 0 - 20 °C / Inert atmosphere
With
thionyl chloride; sulfuric acid; potassium tert-butylate; water; nitric acid; potassium carbonate; acetic acid; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; chloroform; water; N,N-dimethyl-formamide; acetone;
DOI:10.1002/chem.201102732