2-Hydroxy-5-tricyclo[3.3.1.13,7]dec-1-ylbenzoic acid hydrazide

Base Information

Chemical Name:2-Hydroxy-5-tricyclo[3.3.1.13,7]dec-1-ylbenzoic acid hydrazide
CAS No.:126145-53-7
Molecular Formula:C₁₇H₂₂N₂O₂
Molecular Weight:286.374
Hs Code.:
DSSTox Substance ID:DTXSID401178254

Synonyms:DTXSID401178254;2-Hydroxy-5-tricyclo[3.3.1.13,7]dec-1-ylbenzoic acid hydrazide;126145-53-7

Suppliers and Price of 2-Hydroxy-5-tricyclo[3.3.1.13,7]dec-1-ylbenzoic acid hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Hydroxy-5-tricyclo[3.3.1.13,7]dec-1-ylbenzoic acid hydrazide

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:286.168127949
Heavy Atom Count:21
Complexity:395

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C2CC3CC1CC(C2)(C3)C4=CC(=C(C=C4)O)C(=O)NN

Technology Process of 2-Hydroxy-5-tricyclo[3.3.1.13,7]dec-1-ylbenzoic acid hydrazide

There total 4 articles about 2-Hydroxy-5-tricyclo[3.3.1.13,7]dec-1-ylbenzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.01%

: 126145-52-6
methyl 5-(adamantan-1-yl)-2-hydroxybenzoate

: 126145-53-7
5-(adamant-1-yl)salicylic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 10h; Heating;
DOI:10.1007/BF00764444

Reference yield:

: 768-90-1
1-Adamantyl bromide

: 126145-53-7
5-(adamant-1-yl)salicylic acid hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 87.41 percent / H₂O / 0.25 h / 160 - 170 °C

2: 63.78 percent / KOH / H₂O; acetone / 20 h / Ambient temperature

3: 36.01 percent / hydrazine hydrate / ethanol / 10 h / Heating

With potassium hydroxide; water; hydrazine hydrate; In ethanol; water; acetone;
DOI:10.1007/BF00764444

Reference yield:

: 126145-51-5
5-(adamantan-1-yl)-2-hydroxybenzoic acid

: 126145-53-7
5-(adamant-1-yl)salicylic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 63.78 percent / KOH / H₂O; acetone / 20 h / Ambient temperature

2: 36.01 percent / hydrazine hydrate / ethanol / 10 h / Heating

With potassium hydroxide; hydrazine hydrate; In ethanol; water; acetone;
DOI:10.1007/BF00764444