FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂

Base Information

Chemical Name:FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂
CAS No.:950193-44-9
Molecular Formula:C₂₄H₁₇FeNO₂
Molecular Weight:407.251
Hs Code.:

FeC<sub>5</sub>H<sub>5</sub>C<sub>5</sub>H<sub>4</sub>C<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>NO<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂

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Technology Process of FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂

There total 1 articles about FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1271-47-2
ferroceneacetylene

: 29170-08-9
4-iodo-4'-nitrobiphenyl

: 950193-44-9
FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂

Guidance literature:: With catalyst: Pd(PPh₃)2Cl₂/Cu(OAc)2 1:1 mixt.; In diethylamine; Fe-compound and organic ligand stirred in diethylamine in 1:1 molar ratio with Pd-complex and Cu(OAc)2 for 20 h under reflux; solvent removed in vacuum; dissolved in CH2Cl2; concd.; sepd. by column chromy. on neutral alumina eluted with hexane-benzene 10:1 mixt.; recrystalized in hexane-benzene; elem. anal.;
DOI:10.1016/j.poly.2007.02.023

Reference yield: 73.0%

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 950193-44-9
FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂

: 950193-50-7
FeC₅H₅C₅H₄C₂C₆H₄C₆H₄NO₂Co₂(CO)6

Guidance literature:: In benzene; benzene soln. of Fe-compound and Co2(CO)8 in 1:1 molar ratio stirred for0.5 h at 50°C; solvent removed in vacuum; dissolved in benzene; sepd. by column chromy.on silica gel eluted with hexane-benzene 10:1 mixt.; recrystallized fro m hexane-CH2Cl2 at -20°C; elem. anal.;
DOI:10.1016/j.poly.2007.02.023