platinum(4,7-diphenyl-1,10-phenanthroline)(azido)2

Base Information

Chemical Name:platinum(4,7-diphenyl-1,10-phenanthroline)(azido)2
CAS No.:124478-80-4
Molecular Formula:C₂₄H₁₆N₈Pt
Molecular Weight:611.525
Hs Code.:

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Chemical Property of platinum(4,7-diphenyl-1,10-phenanthroline)(azido)2

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Technology Process of platinum(4,7-diphenyl-1,10-phenanthroline)(azido)2

There total 2 articles about platinum(4,7-diphenyl-1,10-phenanthroline)(azido)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 35273-41-7
dichlorido(4,7-diphenyl-1,10-phenanthroline)platinum(II)

: 124478-80-4
platinum(4,7-diphenyl-1,10-phenanthroline)(azido)2

Guidance literature:: With NaN₃; In methanol; N,N-dimethyl-formamide; dropwise addn. of NaN3 in MeOH to the complex in DMF, stirred (4 h); filtered, concd. (water bath, about 50°C), dropwise addn. of MeOH, kept in a refrigerator overnight, crystals filtered, recrystn. (acetone), dried (vac., CaCl2); elem. anal.;
DOI:10.1016/S0020-1693(00)90114-2

Reference yield:

: 1662-01-7
bathophenanthroline

: 124478-80-4
platinum(4,7-diphenyl-1,10-phenanthroline)(azido)2

Guidance literature:: Multi-step reaction with 2 steps

1: NaCl; HCl / water; methanol

2: NaN₃ / N,N-dimethyl-formamide; methanol

With NaCl; HCl; NaN₃; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/S0020-1693(00)90114-2