C₁₀H₁₁FO₂S

Base Information

Chemical Name:C₁₀H₁₁FO₂S
CAS No.:1251164-93-8
Molecular Formula:C₁₀H₁₁FO₂S
Molecular Weight:214.261
Hs Code.:

C<sub>10</sub>H<sub>11</sub>FO<sub>2</sub>S

Synonyms:

Suppliers and Price of C₁₀H₁₁FO₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₁₁FO₂S

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₀H₁₁FO₂S

There total 7 articles about C₁₀H₁₁FO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1251164-92-7
C₉H₈F₂O₂

: 5188-07-8
sodium thiomethoxide

: 1251164-93-8
C₁₀H₁₁FO₂S

Guidance literature:: C₉H₈F₂O₂; With sodium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

sodium thiomethoxide; In dimethyl sulfoxide; at 55 - 60 ℃; for 4h;
DOI:10.1021/jm3007933

Reference yield:

: 1239331-90-8
(2,3-difluorophenyl)-ethyl 4-methylbenzenesulfonate

: 1251164-93-8
C₁₀H₁₁FO₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium bromide / acetone / 3 h / Reflux

2.1: magnesium; ethylene dibromide / diethyl ether / 1.5 h / Reflux

3.1: iron; bromine / chloroform / 20 °C

4.1: isopropylmagnesium bromide / tetrahydrofuran / 24 h / 0 - 20 °C

4.2: 0.67 h / Cooling with ice

5.1: sodium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

5.2: 4 h / 55 - 60 °C

With bromine; isopropylmagnesium bromide; iron; magnesium; ethylene dibromide; lithium bromide; sodium hydroxide; In tetrahydrofuran; diethyl ether; chloroform; dimethyl sulfoxide; acetone;
DOI:10.1021/jm3007933

Reference yield:

: 145689-41-4
2-(2,3-difluorophenyl)acetic acid

: 1251164-93-8
C₁₀H₁₁FO₂S

Guidance literature:: Multi-step reaction with 7 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4 h / Reflux

1.2: 1 h / 0 - 20 °C

2.1: triethylamine / dichloromethane / 5 h / 20 °C

3.1: lithium bromide / acetone / 3 h / Reflux

4.1: magnesium; ethylene dibromide / diethyl ether / 1.5 h / Reflux

5.1: iron; bromine / chloroform / 20 °C

6.1: isopropylmagnesium bromide / tetrahydrofuran / 24 h / 0 - 20 °C

6.2: 0.67 h / Cooling with ice

7.1: sodium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

7.2: 4 h / 55 - 60 °C

With dimethylsulfide borane complex; bromine; isopropylmagnesium bromide; iron; magnesium; ethylene dibromide; triethylamine; lithium bromide; sodium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; acetone;
DOI:10.1021/jm3007933