ethyl 2-acetoxy-β-ionylideneacetate

Base Information

Chemical Name:ethyl 2-acetoxy-β-ionylideneacetate
CAS No.:120674-46-6
Molecular Formula:C₁₉H₂₈O₄
Molecular Weight:320.429
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-acetoxy-β-ionylideneacetate

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Technology Process of ethyl 2-acetoxy-β-ionylideneacetate

There total 2 articles about ethyl 2-acetoxy-β-ionylideneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66465-74-5
4-(5'-hydroxy-2',2',6'-trimethylcyclohex-1'-enyl)but-3-en-2-on

: 120674-46-6
ethyl 2-acetoxy-β-ionylideneacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / DMAP / triethylamine / 2 h / Ambient temperature

2: 1.) 15 percent n-BuLi / 1.) hexane/THF, r. t., 0.5 h, 2.) THF, reflux, 3 h

With dmap; n-butyllithium; In triethylamine;
DOI:10.1248/cpb.36.78

Reference yield:

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 78392-21-9
(E)-2,2,4-trimethyl-3-(3-oxobut-1-en-1-yl)cyclohex-3-en-1-yl acetate

: 120674-64-8
ethyl 2-acetoxy-β-ionylideneacetate

: 120674-46-6
ethyl 2-acetoxy-β-ionylideneacetate

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) hexane/THF, r. t., 0.5 h, 2.) THF, reflux, 3 h;
DOI:10.1248/cpb.36.78