Technology Process of C28H49N2O3(1+)*Br(1-)
There total 4 articles about C28H49N2O3(1+)*Br(1-) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen bromide; bromine / 1,4-dioxane / 0 - 20 °C
2: acetonitrile / Reflux
With
hydrogen bromide; bromine;
In
1,4-dioxane; acetonitrile;
DOI:10.1007/s11743-012-1356-x
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / chloroform / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 65 - 70 °C
3: hydrogen bromide; bromine / 1,4-dioxane / 0 - 20 °C
4: acetonitrile / Reflux
With
hydrogen bromide; bromine; potassium carbonate; triethylamine;
In
1,4-dioxane; chloroform; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1007/s11743-012-1356-x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 65 - 70 °C
2: hydrogen bromide; bromine / 1,4-dioxane / 0 - 20 °C
3: acetonitrile / Reflux
With
hydrogen bromide; bromine; potassium carbonate;
In
1,4-dioxane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1007/s11743-012-1356-x