bis(2-(3,5-dimethyl)phenylaminopyridinato) titanium dichloride complex

Base Information

• Chemical Name: bis(2-(3,5-dimethyl)phenylaminopyridinato) titanium dichloride complex
• CAS No.: 1107661-65-3
• Molecular Formula: C₂₆H₂₆Cl₂N₄Ti
• Molecular Weight: 513.305
• Mol file: 1107661-65-3.mol

Synonyms:

Chemical Property of bis(2-(3,5-dimethyl)phenylaminopyridinato) titanium dichloride complex

Chemical Property:

Purity/Quality:

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Technology Process of bis(2-(3,5-dimethyl)phenylaminopyridinato) titanium dichloride complex

There total 1 articles about bis(2-(3,5-dimethyl)phenylaminopyridinato) titanium dichloride complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

titanium tetrachloride (7550-45-0) + 2-(3',5'-dimethylphenylamino)pyridine (227805-75-6) → bis(2-(3,5-dimethyl)phenylaminopyridinato) titanium dichloride complex (1107661-65-3)

Guidance literature:

With sodium hydride; In diethyl ether; toluene; amidopyridine react with NaH (excess) in dry Et2O at room temp. until nogas evolved, soln. filtered through glass filter, added dropwisely to t oluene soln. of TiCl4, stirred 1 h at room temp.; filtration (Kieselguhr), evapn. under vac., elem. anal.;

DOI:10.1016/j.molcata.2007.10.029

upstream raw materials:

titanium tetrachloride

2-(3',5'-dimethylphenylamino)pyridine