η3-allyl-bis(triphenylphosphite)nickel(II) tetrafluoroborate

Base Information

Chemical Name:η3-allyl-bis(triphenylphosphite)nickel(II) tetrafluoroborate
CAS No.:114367-37-2
Molecular Formula:BF₄*C₃₉H₃₅NiO₆P₂
Molecular Weight:807.145
Hs Code.:

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Chemical Property of η3-allyl-bis(triphenylphosphite)nickel(II) tetrafluoroborate

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Technology Process of η3-allyl-bis(triphenylphosphite)nickel(II) tetrafluoroborate

There total 1 articles about η3-allyl-bis(triphenylphosphite)nickel(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 101-02-0
triphenyl phosphite

: 67969-82-8
tetrafluoroboric acid diethyl ether

: bis(η3-allyl)nickel(II)

: 114367-37-2
η3-allyl-bis(triphenylphosphite)nickel(II) tetrafluoroborate

Guidance literature:: In diethyl ether; Ni(C3H5)2 is dissolved in ether at -25°C, to this soln. P(OPh)3 is added with stirring under Ar, to the mixt. HBF4*OEt2 is added; soln. is allowed to warm to room temp., ppt. is filtered off, washed with ether and dried in vac., residue is recrystd. from CH2Cl2 and ether, elem. anal.;
DOI:10.1016/0022-328X(87)80255-3