1-(2-benzoylthien-5-yl)-1'-(tributylstannyl)ferrocene

Base Information

Chemical Name:1-(2-benzoylthien-5-yl)-1'-(tributylstannyl)ferrocene
CAS No.:400736-14-3
Molecular Formula:C₃₃H₄₂FeOSSn
Molecular Weight:661.319
Hs Code.:

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Chemical Property of 1-(2-benzoylthien-5-yl)-1'-(tributylstannyl)ferrocene

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Technology Process of 1-(2-benzoylthien-5-yl)-1'-(tributylstannyl)ferrocene

There total 1 articles about 1-(2-benzoylthien-5-yl)-1'-(tributylstannyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 31161-46-3
2-benzoyl-5-bromothiophene

: 12291-11-1
1,1'-bis(tri-n-butylstannyl)ferrocene

: 400736-14-3
1-(2-benzoylthien-5-yl)-1'-(tributylstannyl)ferrocene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; to mixt. of Fe-complex and Pd-complex in DMF ligand was added, heated at100-120°C for 1 h, cooled; NH4Cl was added, extd. with petroleum ether or Et2O, washed with satd. KF and water, organic layer was dried on MgSO4, filtered, concd. in vacuo, flash chromy. on Al2O3 with petroleum ether, petroleum ether-Et2O; elem. anal.;
DOI:10.1016/S0022-328X(01)00895-6

Reference yield: 60.0%

: 400736-14-3
1-(2-benzoylthien-5-yl)-1'-(tributylstannyl)ferrocene

: 400736-34-7
1',1'''-bis(2-benzoylthien-5-yl)diferrocene

Guidance literature:: copper(II) sulfate trihydrate; In tetrahydrofuran; CuSO4*3H2O was added to Fe-complex in THF, stirred at ambient temp. for 10 h; diluted with CH2Cl2, washed with aq. NH3, water, brine, dried over MgSO4, concd. in vacuo, column chromy. on silica gel with petroleum ether-MeOH;
DOI:10.1016/S0022-328X(01)00895-6