Technology Process of C22H13ClF3NO4
There total 4 articles about C22H13ClF3NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ammonium chloride; zinc
2: manganese(IV) oxide / dichloromethane / 20 °C
3: pyridine; hydroxylamine hydrochloride / ethanol / Reflux
4: isopropyl alcohol / 4 h / 65 °C / Combinatorial reaction / High throughput screening (HTS)
With
pyridine; manganese(IV) oxide; hydroxylamine hydrochloride; ammonium chloride; zinc;
In
ethanol; dichloromethane; isopropyl alcohol;
DOI:10.1002/asia.201100154
- Guidance literature:
-
Multi-step reaction with 3 steps
1: manganese(IV) oxide / dichloromethane / 20 °C
2: pyridine; hydroxylamine hydrochloride / ethanol / Reflux
3: isopropyl alcohol / 4 h / 65 °C / Combinatorial reaction / High throughput screening (HTS)
With
pyridine; manganese(IV) oxide; hydroxylamine hydrochloride;
In
ethanol; dichloromethane; isopropyl alcohol;
DOI:10.1002/asia.201100154
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; hydroxylamine hydrochloride / ethanol / Reflux
2: isopropyl alcohol / 4 h / 65 °C / Combinatorial reaction / High throughput screening (HTS)
With
pyridine; hydroxylamine hydrochloride;
In
ethanol; isopropyl alcohol;
DOI:10.1002/asia.201100154