Technology Process of C26H32N2O3S2
There total 14 articles about C26H32N2O3S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
2: Lawessons reagent; pyridine / toluene / 100 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran
4: thionyl chloride / toluene
5: N-ethyl-N,N-diisopropylamine / acetonitrile
6: water; sodium hydroxide / ethanol
With
Lawessons reagent; pyridine; thionyl chloride; tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 10 steps
1: aluminum (III) chloride
2: sodium hydride
3: PhMe2NBr3
4: sodium diformamide
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
6: Lawessons reagent; pyridine / toluene / 100 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran
8: thionyl chloride / toluene
9: N-ethyl-N,N-diisopropylamine / acetonitrile
10: water; sodium hydroxide / ethanol
With
Lawessons reagent; pyridine; aluminum (III) chloride; thionyl chloride; sodium diformamide; tetrabutyl ammonium fluoride; water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 1H-imidazole
2: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)
3: n-butyllithium / tetrahydrofuran
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
5: Lawessons reagent; pyridine / toluene / 100 °C
6: tetrabutyl ammonium fluoride / tetrahydrofuran
7: thionyl chloride / toluene
8: N-ethyl-N,N-diisopropylamine / acetonitrile
9: water; sodium hydroxide / ethanol
With
Lawessons reagent; pyridine; 1H-imidazole; n-butyllithium; thionyl chloride; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067