2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester

Base Information

• Chemical Name: 2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester
• CAS No.: 89435-84-7
• Molecular Formula: C₃₃H₃₃N₃O₈S
• Molecular Weight: 631.706

Synonyms:

Chemical Property of 2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester

Chemical Property:

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Safty Information:

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Useful:

Technology Process of 2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester

There total 3 articles about 2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → 2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester (89435-84-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / CH₂Cl₂

With potassium carbonate; In dichloromethane;

Reference yield:

2-((2R,3R)-3-Amino-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester (31925-12-9) → 2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester (89435-84-7)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / CH₂Cl₂

With potassium carbonate; In dichloromethane;

Reference yield:

para-nitrobenzyl malonyl chloride (89435-83-6) + 2-((2R,3R)-3-Benzylamino-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester (89435-82-5) → 2-((2R,3R)-3-{Benzyl-[2-(4-nitro-benzyloxycarbonyl)-acetyl]-amino}-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester (89435-84-7)

Guidance literature:

upstream raw materials:

para-nitrobenzyl malonyl chloride

2-((2R,3R)-3-Benzylamino-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester

benzyl bromide

2-((2R,3R)-3-Amino-2-methylsulfanyl-4-oxo-azetidin-1-yl)-3-methyl-but-2-enoic acid benzyl ester

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